Optical Studies of Single Molecules and Molecular Assemblies in Chemical Physics and Biophysics

PHYS division symposium

ACS National Meeting, San Diego, CA, April 1-5, 2001

 

Organizers

 

Anne Myers Kelley (Kansas State University) amkelley@ksu.edu, tel. 785-532-3843

Shimon Weiss (Lawrence Berkeley National Laboratory) sweiss@lbl.gov, tel. 510-486-5202

 

 

Until quite recently, essentially all physical measurements on molecular-scale entities involved averaging over large ensembles.  The ability to interrogate individual molecules and molecular assemblies on a one-by-one basis is driving revolutionary changes in our understanding of fundamental chemical and biological processes.  This symposium will focus on optical probes (fluorescence, absorption, Raman, and nonlinear spectroscopies) of the chemical physics and biophysics of molecules and supramolecular structures in which single-molecule techniques can reveal important heterogeneities hidden in traditional ensemble measurements.  Systems of interest include single molecules in liquids and solids and on surfaces, metallic and semiconductor nanoparticles, J-aggregates, conducting polymers, molecularly doped sol-gels, single molecules in biomembranes, single peptides, enzymes, structural and motor proteins, single oligonucleotides, DNAs, and RNAs, and single photosynthetic reaction centers. 

 

Supported by:

 

Becker & Hickl GmbH,  Carl Zeiss,  Roper Scientific,  PicoQuant GmbH,  Coherent, Inc.

 

 

Invited speakers:

 

Sunney Xie (Dept. of Chemistry and Chemical Biology, Harvard Univ., Cambridge, MA; xie@chemistry. harvard.edu) Single-Molecule Enzymatic and Conformational Dynamics

 

W.E. Moerner  (Dept. of Chemistry, Stanford Univ., Stanford, CA; w.e.moerner@stanford.edu) “Single-molecule spectroscopy, from quantum optics to molecular motors”

 

Robin Hochstrasser (Dept. of Chemistry, Univ. of Pennsylvania, Philadelphia, PA; hochstra@sas.upenn.edu)  “Equilibrium fluctuations and energy transfer of reactions and conformational dynamics of proteins”

 

• Kazuhiko Kinosita Jr. (Department of Physics, Faculty of Science and Technology, Keio University, Yokohama, Japan; kazuhiko@phys.keio.ac.jp) “Optical imaging of rotary molecular motors”

 

• Toshio Yanagida (Dept. of Physiology and Biosignaling, Osaka University School of Medicine, Osaka, Japan; yanagida@bpe.osaka-u.ac.jp) “Single molecule biophysics”

 

Thomas Schmidt (Leiden Institute of Physics, Leiden University, Leiden, The Netherlands; tschmidt@biophys.leidenuniv.nl) “Single-molecule imaging for the study of biological membranes”

 

Claus Seidel (Max-Planck-Institut für Biophysikalische Chemie, Am Fassberg 11, D-37077 Göttingen, Germany; cseidel@gwdg.de) “Analysis of molecular structure and dynamics by selective single-molecule fluorescence spectroscopy”

 

Markus Sauer (Physikalisch-Chemisches Institut, Universität Heidelberg, Heidelberg, Germany; sauer@urz.uni-heidelberg.de) “Spectrally-resolved fluorescence lifetime imaging of single molecules”

 

• Jan Schmidt (Huygens Laboratory, Centre of the Study of Excited States of Molecules, Leiden University, Leiden, The Netherlands; mat@molphys.leidenuniv.nl) “Single-molecule spectroscopic studies of light-harvesting complexes of photosynthetic bacteria”

 

Michel Orrit (C.P.M.O.H., CNRS et Université Bordeaux I, Talence, France; orrit@yak.cpmoh.u-bordeaux.fr)  Dynamics of solids at low temperatures studied with single molecules”

 

Paul Barbara (Dept. of Chemistry, University of Texas, Austin TX; p.barbara@mail.utexas.edu) “Single molecule spectroscopy of conjugated polymers”

 

Ed Yeung (Department of Chemistry, Iowa State University, Ames, IA; yeung@ameslab.gov) “Single-molecule disease diagnosis based on electrophoresis and spectroscopy”

 

• Christian G. Hübner representing group of Urs Wild (Laboratorium für Physikalische Chemie, ETH-Zentrum, Zürich, Switzerland; wild@phys.chem.ethz.ch) “Direct observation of the influence of oxygen on the singlet and triplet lifetime of single dye molecules”

Thomas Basché (Institut fuer Physikalische Chemie, Johannes Gutenberg-Universität, Mainz, Germany; thomas.basche@uni-mainz.de) “Confocal fluorescence and Raman spectroscopy of single nanoparticles”

 

Katrin Kneipp (Technical University of Berlin, Physics Department, Berlin, Germany, and MIT; Kneipp@usa.net) “Ultrasensitive Raman spectroscopy at the single molecule level based on surface-enhanced Raman scattering on silver and gold colloidal clusters”

 

Bob Dunn (Dept. of Chemistry, University of Kansas, Lawrence, KS; rdunn@caco3.chem.ukans.edu) “Single molecule studies of artificial pulmonary lung surfactant”

 

Dan Higgins (Dept. of Chemistry, Kansas State University, Manhattan, KS; higgins@ksu.edu) “Molecular scale environments in organic and inorganic composite films probed by single molecule spectroscopy”

 

Shuming Nie (Department of Chemistry, Indiana University, Blooomington, IN; nie@indiana.edu) “Probing single molecules and single nanoparticles by surface-enhanced Raman scattering”

 

Peter Wolynes (Department of Chemistry, University of Illinois, Urbana, IL  61801; wolynes@scs.uiuc.edu) Intermittency of Activated Events in Single Molecules

 

Rob Dickson (School of Chemistry and Biochemistry, Georgia Institute of Technology, Atlanta, GA; dickson@chemistry.gatech.edu) “Three-dimensional single molecule orientational microscopy and dynamics”

 

• Kurt Thorn representing group of Ron Vale (Dept. of Pharmacology, University of California, San Francisco, CA; vale@phy.ucsf.edu, thorn@itsa.ucsf.edu) “Deciphering kinesin motility with single molecule microscopy”

 

Norman Dovichi (Dept. of Chemistry, University of Alberta, Edmonton, Alberta, Canada; norm.dovichi@ualberta.ca) “Michaelis-Menten kinetics of a single molecule of calf-intestinal alkaline phosphatase”

 

• Mikael Käll (Dept. of Applied Physics, Chalmers University of Technology, Göteborg, Sweden; kall@fy.chalmers.se) “Inhomogeneous broadening and single molecule fine-structure in surface-enhanced Raman spectra of proteins and amino acids”

 

Eitan Geva (Dept. of Chemistry, Univ. of Michigan, Ann Arbor, Michigan; eitan@umich.edu) “Single molecule spectroscopy in glasses”

 

Louis Brus (Dept. of Chemistry, Columbia University, New York, NY; brus@chem.columbia.edu) “Raman spectra of single R6G molecules on Ag nanocrystal aggregates”

 

Jörg Wrachtrup (Institute der Physik, Universität Stuttgart, Stuttgart, Germany; j.wrachtrup@physik.uni-stuttgart.de )Observation of charge and energy transfer in single photosynthetic reaction centers”

 

Steven Chu (Dept. of Physics, Stanford Univ., Stanford, CA; schu@stanford.edu) “Single molecule fluorescence studies of ribozymes and proteins”

 

 

 

 

Final schedule of oral presentations

San Diego Marriott

 

Sunday morning (Chair, Thomas Basché)

 

8:20 — 1. Deciphering kinesin motility with single molecule microscopy. K. S. Thorn, M. Tomishige, R. D. Vale

9:00 — 2. Optical imaging of rotary molecular motors. K. Kinosita Jr.

9:40 — 3. Observation of a single dye labeled virus on its infectious entry pathway into a living cell. C. Bräuchle

10:00 — Intermission.

10:20 — 4. Single molecule biophysics. T. Yanagida

11:00 — 5. Single-molecule spectroscopy, from quantum optics to molecular motors W. E. Moerner, B. Lounis, H. Sosa, E. J. G. Peterman, L. S. B. Goldstein

11:40 — 6. Single-molecule dynamics and interactions at living interfaces. X. N. Xu, R. Jeffers, S. Huang, D. Wang, M. Nowak

 

 

Sunday afternoon (Chair, W.E. Moerner)

 

1:40 — 23. Michaelis-Menten kinetics of a single molecule of calf-intestinal alkaline phosphatase. N. J. Dovichi, R. Polakowski, M. Eggerston

2:20 — 24. Single-molecule enzymatic and conformational dynamics. X. S. Xie

3:00 — 25. Conformational substates dynamics in the active adrenergic receptor. G. Peleg, P. Ghanouni, B. K. Kobilka, R. N. Zare

3:20 — Intermission.

3:40 — 26. Spectrally-resolved fluorescence lifetime imaging of single molecules. M. Sauer

4:20 — 27. New tools for single molecule dynamics: From trapping in vesicles to surface enhanced Raman scattering. G. Haran, E. Boukobza, A. Weiss

4:40 — 28. Simultaneous "dual-color and dual-polarization imaging" as a tool for co-localization and fluorescence resonant energy transfer studies of single molecules. G. Harms, L. Cognet, G. A. Blab, P. H. M. Lommerse, T. Schmidt

5:00 — 29. Single-molecule spectroscopy study of the mechanisms and dynamics of molecular interactions and enzymatic reactions. H. P. Lu, Y. Chen

 

 

Monday morning (Chair, Anne Kelley)

 

8:20 — 49. Dynamics of solids at low temperatures studied with single molecules. J. Caruge, M. Orrit

9:00 — 50. Single molecule spectroscopy in glasses. E. Geva, J. L. Skinner

9:40 — 51. Fluctuation in single molecule spectroscopy. Y. Jung, E. Barkai, R. J. Silbey

10:00 — Intermission.

10:20 — 52. Confocal fluorescence and Raman spectroscopy of single nanoparticles. T. Basché, A. Mews

11:00 — 53. Spectroscopy of single Si nanoparticles. S. K. Buratto, M. D. Mason, P. J. Carson, G. M. Credo

11:20 — 54. Photon antibunching in the fluorescence of single molecules embedded in a thin polymer film. F. Treussart, C. Grossman, R. Pansu, J. Roch

11:40 — 55. Non-Lorentzian spectral line shapes of single molecules: Beyond the sudden jump model. T. Plakhotnik

 

 

Monday afternoon (Chair, Anne Kelley)

 

1:40 — 80. Analysis of molecular structure and dynamics by selective single-molecule fluorescence spectroscopy. C. A. M. Seidel, E. Schweinberger, S. Berger, C. Eggeling, J. Schaffer, J. Widengren, S. Felekyan

2:20 — 81. Single molecule fluorescence studies of ribozymes and proteins. S. Chu

3:00 — 82. Single-molecule imaging and time-resolved fluorometry of an analog of adenine. M. Ishikawa, J. Ye

3:20 — Intermission.

3:40 — 83. Single-molecule disease diagnosis based on electrophoresis and spectroscopy. E. S. Yeung, M. R. Shortreed, Y. Ma, S. H. Kang, H. Li

4:20 — 84. Single-molecule imaging for the study of biological membranes. T. Schmidt

5:00 — 85. Theoretical studies of room-temperature single molecule experiments. J. Cao

 

 

Tuesday morning (Chair, Michel Orrit)

 

8:20 — 109. Inhomogeneous broadening and single molecule fine-structure in surface-enhanced Raman spectra of proteins and amino acids. M. Käll, E. J. Bjerneld, H. Xu, P. Johansson

9:00 — 110. Probing single molecules and single nanoparticles by surface-enhanced Raman scattering. S. Nie

9:40 — 111. Correlation of SERS activity and micro-structure of silver colloids. Y. Maruyama, M. Ishikawa, M. Futamata

10:00 — Intermission.

10:20 — 112. Raman spectra of single R6G molecules on Ag nanocrystal aggregates. L. Brus

11:00 — 113. Ultrasensitive Raman spectroscopy at the single molecule level based on surface-enhanced Raman scattering on silver and gold colloidal clusters. K. Kneipp, H. Kneipp, I. Itzkan, R. R. Dasari, M. S. Feld

11:40 — 114. Photoactivated fluorescence from individual silver nanoclusters. L. A. Peyser, A. E. Vinson, A. P. Bartko, R. M. Dickson

 

 

Wednesday morning (Chair, Dan Higgins)

 

8:20 — 143. Single molecule studies of artificial pulmonary lung surfactant. B. N. Flanders, S. A. Vickery, R. C. Dunn

9:00 — 144. 3-D Single molecule orientational microscopy and dynamics. R. M. Dickson

9:40 — 145. Probing surface diffusion heterogeneity at biomaterial interfaces with single-event histograms. D. L. Burden, S. D. Poppen, J. T. Elliott, J. T. Woodward, A. Sehgal

10:00 — Intermission.

10:20 — 146. Direct observation of the influence of oxygen on the singlet and triplet lifetime of single dye molecules. C. G. Hübner, I. Renge, A. Renn, U. P. Wild

11:00 — 147. Lateral diffusion of non-tethered phospholipids in polymer-tethered phospholipid membranes studied at the single molecule level. C. A. Naumann, P. C. Ke

11:20 — 148. Single molecule studies of heterogeneous dynamics near the glass transition. L. A. Deschenes, D. A. Vanden Bout

11:40 — 149. Time resolved fluorescence spectroscopy on the photo-physical behavior of single molecules and quantum dots. P. L. T. M. Frederix, W. G. J. H. M. Van Sark, D. J. Van den Heuvel, E. L. De Beer, H. C. Gerritsen

 

 

Wednesday afternoon (Chair, Steve Buratto)

 

1:40 — 173. Molecular scale environments in organic and inorganic composite films probed by single molecule spectroscopy. D. A. Higgins, M. M. Collinson, A. M. Bardo, E. Mei, Y. Hou, R. Allenbaugh, S. Ginagunta

2:20 — 174. Single molecule spectroscopy of conjugated polymers. P. F. Barbara, D. Hu, J. Yu, N. W. Song

3:00 — 175. Single molecule probing of nanoscale polymer dynamics. M. F. Garcia-Parajo, J. A. Veerman, R. Bouwhuis, R. Vallee, J. G. Vancso, N. F. van Hulst

3:20 — Intermission.

3:40 — 176. Intermittency of activated events in single molecules. P. Wolynes

4:20 — 177. Imaging the excitation profile of a confocal microscope for correlated fluorescence/AFM of individual nanosized particles and biomolecules. A. Van Orden, D. Willard, L. Kolodny, L. Carillo, M. Nelson

4:40 — 178. Probing single-ion luminescence in rare-earth doped nanocrystals. M. D. Barnes, A. Mehta, T. Thundat, R. Bhargava

5:00 — 179. Excitons and polaritons in individual J-aggregate fibers and organic-inorganic CdSe nanocrystal systems. M. Vacha, S. Takei, H. Suzuki, K. Hashizume, M. Furuki, L. S. Pu, T. Tani

 

 

Thursday morning (Chair, Shimon Weiss)

 

8:20 — 356. Observation of charge and energy transfer in single photosynthetic reaction centers. J. Wrachtrup, F. Jelezko, C. Tietz

9:00 — 357. Single-molecule spectroscopic studies of light-harvesting complexes of photosynthetic bacteria. J. Schmidt

9:40 — 358. Energy transfer studies of single phycoerythrocyanin molecules. P. Zehetmayer, H. Scheer, C. Bräuchle, A. Zumbusch

10:00 — Intermission.

10:20 — 359. Equilibrium fluctuations and energy transfer of reactions and conformational dynamics of proteins. R. M. Hochstrasser, E. Mei, J. Tang, M. Lee

11:00 — 360. Multichromophoric dendrimers: Model systems for the study of energy transfer processes in antenna systems. F. C. De Schryver, J. Hofkens

11:20 — 361. Hidden Markov models applied to time correlated single photon trajectories of single molecules. D. S. Talaga

11:40 — 362. NSOM measurements of single human retinal lipofuscin granules. J. D. Simon, L. E. Lamb, R. C. Dunn, J. R. Krogmeier, T. Sarna, C. M. R. Clancy, N. M. Haralampus-Grynaviski, A. Pawlak, M. Rozanowska

 

 

Thursday afternoon (Chair, Rob Dickson)

1:40 — 379. Single molecule studies of living colors and transmembrane proteins on cells. M. F. Garcia-Parajo, B. I. de Bakker, M. Koopman, C. Figdor, N. F. van Hulst

2:00 — 380. Phonon-assisted exciton delocalization in 1-D biological antenna complexes. Z. G. Yu, X. Song.  Withdrawn.

2:20 — 381. Single molecule rotational mobility in glassy state polymers. A. P. Bartko, R. M. Dickson

2:40 — Intermission.

3:00 — 382. Observation of single molecule diffusion in liquids near interfaces. J. Schuster, F. Cichos, J. Wrachtrup, C. von Borczyskowski

3:20 — 383. Luminescence lifetimes of single molecules in disordered media. T. Plakhotnik, E. A. Donley

3:40 — 384. Submicron structure of a Shpol'skii matrix: A single-molecule study of dibenzanthanthrene in n-tetradecane. A. Bloeß, Y. Durand, M. Matsushita, E. J. J. Groenen, J. Schmidt